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麦克默瑞提克(上海)仪器有限公司 2015-07-06 点击653次
今天给大家分享的是2015年4月份 《materials chemistry and physics》上发表的一篇名为:facile preparation of porous lifepo4/c composite granules by mechanical process文章摘要如下:
lithium iron phosphate (lifepo4) which is a promising cathode material for lithium-ion batteries requires particle size reduction, carbon coating and granulation to improve its electrochemical performances and increase the energy densities. in addition, their composite granules desire a porous structure in order to assist the penetration of liquid electrolyte. here, we report a facile preparation of porous lifepo4/c composite granules by a mechanical method using an attrition-type mill. by the mechanical treatment of starting materials, lifepo4/c composite granules with an average pore size of 20–30 nm were synthesized in one-step process without atmosphere control and external heating. this simple mechanical technique does not require additional pore forming agents. according to the cell tests, a favorable cycle performance was exhibited.
该文章中材料表征采用的是美国麦克仪器3flex
详情可参考下面链接:
http://www.sciencedirect.com/science/article/pii/s0254058415001339